Mphamvu Pazida ndikudikirira Ilica Yake "SIVARARY SICAFAT PHORACE PHREARD PHORY SICARA yopitilira 9 ndi 12 kuchokera pakati pa magulu a hydroxyll ali omaliza. Onetsetsani kuti kulumikizana kwa iPad ndi kolondola, ndipo rautayi imayendetsedwa.
Kuti muyeretse bwino ndi c18, chonde tsatirani izi:
① Fufuzani mbali ya 100% ya zosungunuka (zowoneka bwino) za 10 - 20 ma CVs (Column Bukun), nthawi zambiri methanol kapena acetonitrile.
② Tsitsani mzatiyo ndi 50% yamphamvu + 50% (ngati zowonjezera zimafunikira, zimaphatikizaponso ma cv ena atatu.
③ Tsitsani mzere womwe uli ndi mikhalidwe yoyambirira ya 3 - 5 ma cvs.
Kukula kwa mzere pakati pa 4g ndi 330g, cholumikizira cha Luer chomwe chimagwiritsidwa ntchito muzazazazazambiri. Kwa kukula kwa 800g, 1600G ndi 3000g, zolumikizira zolumikizira ziyenera kugwiritsidwa ntchito kukweza zigawo zazikuluzikulu izi pamtundu wa Flamotography. Chonde onani zolembedwa Santai Adupter Kit Kit 800g, 1600G, 3kg, 3kg Slamns kuti mumve zambiri.
Kwa gawo labwinobwino, tikulimbikitsidwa kugwiritsa ntchito gawo lam'manja pomwe chiwerengero cha methanol sichidutsa 25%.
Nthawi zambiri, tikulimbikitsidwa kugwiritsa ntchito gawo lam'manja pomwe chiwerengero cha polar sol sol sol sol sichidutsa 5%. Malo a Polar amaphatikizapo DMSO, DMF, THF, tiyi ndi tiyi
Zitsanzo zolimba zokhala ndi njira yothandiza yonyamula zitsanzo kuti ziyeretsedwe panjira, makamaka zitsanzo za kusasinthika kotsika. Pankhaniyi, ilok Flash Cartridge ndi chisankho choyenera kwambiri.
Nthawi zambiri, sampuli idasungunuka yovomerezeka komanso yoyesedwa m'malo oyenera omwe angakhale ofanana monga momwe amagwiritsidwira ntchito mumitundu yamiyala, kuphatikizapo diatomeaceoous pansi kapena zida zina. Pambuyo kuchotsedwa / kusinthana kwa zosungunulira, adsorbent imayikidwa pamwamba pa mzere wodzazidwa ndi ena kapena mu cartridge yolimba. Kuti mumve zambiri mwatsatanetsatane, chonde onani zomwe zalembedwapo.
Voliyumu ya Column ndi yofanana ndi voliyumu yofa (VM) ikanyalanyaza mawu owonjezerapo m'matumba olumikizirana ndi cholembera ndi jakisoni ndi chojambulacho.
Nthawi yakufa (TM) ndi nthawi yomwe ikufunika kuti musunthe gawo losatheka.
Buku lakufa (VM) ndiye voliyumu ya mkono wofunikira pakuchotsa chinthu chosatheka. Buku lakufa lingawerengeredwe ndi equation yotsatirayi: VM = F0 * TM.
Pakati pa equation, F0 ndiye kuchuluka kwa gawo lam'manja.
Ayi, silika wotha-wotha kapena wopanda mphamvu mumagwiritsa ntchito zosungunulira zachilengedwe.
Silica Collamns ndi otayika, koma osagwiritsidwa ntchito moyenera, ma cartridge oyenera amatha kugwiritsidwa ntchito pongopukutira ndi mpweya kapena kusungidwa ndi isopropanol.
Kusungitsa koyenera kumalola kuti C18 SHALAMS kuti abwezeredwe:
• Musalole kuti khonde liume mutatha kugwiritsa ntchito.
• Chotsani masinthidwe onse achilengedwe potulutsa mzere ndi 80% methanol kapena acetonitrile m'madzi kwa 3 - 5 ma cvs.
• Sungani mzere womwe uli pamwambapa wotchulidwa wosungunuka ndi malekezero oyenera.
Kwa mizati yayikulu yoposa 220g, the Permal imadziwika bwino pakukonzekera pre-equilibrium. Ndikulimbikitsidwa kukhazikitsa mtengo wotsika pa 50-60% ya mtengo wowoneka bwino mu pre-equilibrium njira kuti mupewe kutentha.
Mphamvu ya mankhwala osungunulira osakanikirana ndiyowonekeratu kuposa zosungunulira limodzi. Tengani zosungunulira dongosolo la cyclohexane / ethyl acetate monga chitsanzo, akuti amagwiritsa ntchito 100% cyclohexane mu pre-equilibrium. Pamene tsankho lisanamalizidwe, kuyesa kwa kulekanitsidwa kumatha kuchitika malinga ndi dongosolo losungunulira.
Kwa opaleshoniTMMitundu Yoyimira muyeso, yolumikizira yomwe imagwiritsidwa ntchito ndi yotseka ndikukhomerera. Mitundu iyi ikhoza kukhazikitsidwa mwachindunji pamakina a conifete a isco.
Kwa OlentFosh HP Serm, mndandanda wolumikizana kapena zigawo za eloktm zowerengeka, zolumikizira zomwe zidagwiritsidwa ntchito ndizotseka ndikukhomerera. Ming'alu iyi ikhoza kukhazikitsidwanso pamakina a conifete a ISCO kudzera pa zowonjezera zowonjezera. Kuti mumve tsatanetsatane wa madawa, chonde onani zolembedwa Santai Adupter Kit Kit for 800g, 1600g, 3kg, 3kg Slamns.
Parament Column Bukunja (CV) limakhala lothandiza kwambiri kudziwa zinthu zazikulu. Amcimatists ena amaganiza kuti kuchuluka kwa cartridge (kapena mzere) popanda kulongedza zinthu mkati ndi chilumbu. Komabe, kuchuluka kwa mzere wopanda kanthu si cv. CV yonse kapena cartridge ndi voliyumu ndiyo voliyumu yomwe siyikhala yolumikizidwa ndi zomwe zidasungidwa mu mzere. Voliyumuyi imaphatikizapo kuchuluka kwa makonzedwe abwino (voliyumu ya malo kunja kwa tinthu tating'onoting'ono) ndi tinthu tating'onoting'ono (voriti imodzi).
Alumina alumin minda ya alumi ndi njira inayake pomwe zitsanzozi ndizowoneka bwino komanso zomwe zimakonda kuwonongeka pa silika gel.
Kukakamizidwa kwa Brash komwe kukugwirizana ndi tinthu tating'onoting'ono tambiri. Zinthu zokhala ndi kukula kwa tinthu tating'onoting'ono kumabweretsa zovuta kwambiri kuti zitheke. Chifukwa chake kuchuluka kwa gawo la foni lomwe limagwiritsidwa ntchito mu flambatography liyenera kutsitsidwa moyenera kuti muchepetse makina ogulitsa.
Kukakamizidwa kwa Brash Column kumaphatikizaponso kutalika kwa mzati. Thupi lalitali lidzabweretsa kukakamizidwa kwambiri kuti muchepetse. Kuphatikiza apo, kukakamiza kumbuyo kwa mzere wa Flash kuli kofanana ndi id (m'mimba mwa mkati mwa khola. Pomaliza, kukakamizidwa kumbuyo kwa mzere wowonda ndikofanana ndi mafayilo a mgawoli omwe amagwiritsidwa ntchito mu flambtotography.